Mechanochemical synthesis of phthalimides with crystal structures of intermediates and products

Melwin Olivier Colaco; Jean Dubois; Johan Wouters

doi:10.1039/c5ce00038f

Mechanochemical synthesis of phthalimides with crystal structures of intermediates and products

Melwin Olivier Colaco, Jean Dubois, Johan Wouters

Unit of theoretical and structural physico-chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

A series of phthalimides have been successfully synthesized in the solid state by grinding (or kneading) of substituted phthalic anhydride and aniline derivatives. Selected products and intermediates were crystallized and characterized by crystallography leading to a potential rationale for the solid-state reactivity that suggests that co-crystals could serve as intermediates. This journal is

Original language	English
Pages (from-to)	2523-2528
Number of pages	6
Journal	CrystEngComm
Volume	17
Issue number	12
DOIs	https://doi.org/10.1039/c5ce00038f
Publication status	Published - 28 Mar 2015

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10.1039/c5ce00038f

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title = "Mechanochemical synthesis of phthalimides with crystal structures of intermediates and products",

abstract = "A series of phthalimides have been successfully synthesized in the solid state by grinding (or kneading) of substituted phthalic anhydride and aniline derivatives. Selected products and intermediates were crystallized and characterized by crystallography leading to a potential rationale for the solid-state reactivity that suggests that co-crystals could serve as intermediates. This journal is",

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AU - Dubois, Jean

AU - Wouters, Johan

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AB - A series of phthalimides have been successfully synthesized in the solid state by grinding (or kneading) of substituted phthalic anhydride and aniline derivatives. Selected products and intermediates were crystallized and characterized by crystallography leading to a potential rationale for the solid-state reactivity that suggests that co-crystals could serve as intermediates. This journal is

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Mechanochemical synthesis of phthalimides with crystal structures of intermediates and products

Abstract

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Physical Chemistry and characterization(PC2)

CCDC 1021628: Experimental Crystal Structure Determination

CCDC 1021629: Experimental Crystal Structure Determination

CCDC 1021632: Experimental Crystal Structure Determination

Cite this

Mechanochemical synthesis of phthalimides with crystal structures of intermediates and products

Abstract

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Equipment

Physical Chemistry and characterization(PC2)

Datasets

CCDC 1021628: Experimental Crystal Structure Determination

CCDC 1021629: Experimental Crystal Structure Determination

CCDC 1021632: Experimental Crystal Structure Determination

Cite this