Résumé
langue originale | Anglais |
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Nombre de pages | 8 |
journal | Crystals |
Volume | 6 |
Les DOIs | |
état | Publié - 21 nov. 2016 |
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Synthesis and Crystallographic Characterization of a Maleimide Derivative of Tryptamine. / Dubois, Jean; Colaço, Melwin; Rondelet, Grégoire; Wouters, Johan (Promoteur).
Dans: Crystals, Vol 6, 21.11.2016.Résultats de recherche: Contribution à un journal/une revue › Article
TY - JOUR
T1 - Synthesis and Crystallographic Characterization of a Maleimide Derivative of Tryptamine
AU - Dubois, Jean
AU - Colaço, Melwin
AU - Rondelet, Grégoire
A2 - Wouters, Johan
PY - 2016/11/21
Y1 - 2016/11/21
N2 - While mechanosynthesis of the target compound, 1-[2-(1H-indol-3-yl)-ethyl]-pyrrole-2,5-dione, C14 H12 N2 O2, did not yield the desired product, it instead resulted in an open intermediate. On the other hand, synthesis starting from the activated maleic anhydride yielded the final maleimide compound. The outcome of the mechanosynthesis has been evaluated by powder X-ray diffraction, and structures of both the final product and open intermediate have been confirmed using single-crystal crystallography.
AB - While mechanosynthesis of the target compound, 1-[2-(1H-indol-3-yl)-ethyl]-pyrrole-2,5-dione, C14 H12 N2 O2, did not yield the desired product, it instead resulted in an open intermediate. On the other hand, synthesis starting from the activated maleic anhydride yielded the final maleimide compound. The outcome of the mechanosynthesis has been evaluated by powder X-ray diffraction, and structures of both the final product and open intermediate have been confirmed using single-crystal crystallography.
KW - mechanosynthesis
KW - grinding
KW - single-crystal structure
KW - powder X-ray diffraction
KW - maleic anhydride
KW - tryptamine
U2 - 10.3390/cryst6110153
DO - 10.3390/cryst6110153
M3 - Article
VL - 6
JO - Crystals
JF - Crystals
SN - 2073-4352
ER -