TY - JOUR
T1 - Preparations of nano-particles, nano-composites and fibers of ZnO from an amide precursor
T2 - Photocatalytic decomposition of (CH)S in a continuous flow reactor
AU - Daniele, S.
AU - Ghazzal, M.N.
AU - Hubert-Pfalzgraf, L.G.
AU - Duchamp, C.
AU - Guillard, C.
AU - Ledoux, G.
PY - 2006/12/14
Y1 - 2006/12/14
N2 - High surface area hexagonal ZnO nano-particles were obtained at room temperature from hydrolysis of the amide derivative Zn[N(SiMe)]. The same procedure applied on silica or cellulose substrates led to homogeneous crack-free hybrid materials for which micro- down to nano-meter replication into ZnO cloth was achieved by calcination at 700 °C. These materials were characterized by FT-IR, UV-vis, photoluminescence, X-ray diffraction (XRD) and transmission electron microscopy (TEM). They demonstrated enhanced photocatalytic degradation of a tough pollutant such as CHSSCH compared with commercial ZnO powder.
AB - High surface area hexagonal ZnO nano-particles were obtained at room temperature from hydrolysis of the amide derivative Zn[N(SiMe)]. The same procedure applied on silica or cellulose substrates led to homogeneous crack-free hybrid materials for which micro- down to nano-meter replication into ZnO cloth was achieved by calcination at 700 °C. These materials were characterized by FT-IR, UV-vis, photoluminescence, X-ray diffraction (XRD) and transmission electron microscopy (TEM). They demonstrated enhanced photocatalytic degradation of a tough pollutant such as CHSSCH compared with commercial ZnO powder.
UR - http://www.scopus.com/inward/record.url?scp=33750524822&partnerID=8YFLogxK
U2 - 10.1016/j.materresbull.2006.04.041
DO - 10.1016/j.materresbull.2006.04.041
M3 - Article
AN - SCOPUS:33750524822
SN - 0025-5408
VL - 41
SP - 2210
EP - 2218
JO - Materials Research Bulletin
JF - Materials Research Bulletin
IS - 12
ER -