Nanoporous solvate of N,N-phthaloyl-glycine

N. A. Tumanov, N. A. Pankrushina, A. A. Nefedov, E. V. Boldyreva

Résultats de recherche: Contribution à un journal/une revueArticle

Résumé

N,N-phthaloyl-glycine is synthesized under microwave activation without solvent. Its nanoporous solvate is obtained by recrystallization. The solvate is studied by single crystal and powder XRD, thermogravimetry, and mass spectrometry. The crystals are composed of dimers that form a framework structure with infinite channels of about 4 Å in diameter, containing a non-stoichiometric amount of chloroform (the mole fraction is close to 0.35). The nature of the incorporated solvate molecules is determined by high-resolution mass spectrometry, and their quantity is found by thermogravimetry. Original Russian Text

langue originaleAnglais
Pages (de - à)606-609
Nombre de pages4
journalJournal of Structural Chemistry
Volume53
Numéro de publication3
Les DOIs
étatPublié - mai 2012
Modification externeOui

Empreinte digitale

glycine
thermogravimetry
Mass spectrometry
Thermogravimetric analysis
Amino acids
mass spectroscopy
Chloroform
Chlorine compounds
chloroform
Dimers
Powders
spectroscopy
Chemical activation
Microwaves
dimers
Single crystals
activation
microwaves
Crystals
Molecules

Citer ceci

Tumanov, N. A. ; Pankrushina, N. A. ; Nefedov, A. A. ; Boldyreva, E. V. / Nanoporous solvate of N,N-phthaloyl-glycine. Dans: Journal of Structural Chemistry. 2012 ; Vol 53, Numéro 3. p. 606-609.
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abstract = "N,N-phthaloyl-glycine is synthesized under microwave activation without solvent. Its nanoporous solvate is obtained by recrystallization. The solvate is studied by single crystal and powder XRD, thermogravimetry, and mass spectrometry. The crystals are composed of dimers that form a framework structure with infinite channels of about 4 {\AA} in diameter, containing a non-stoichiometric amount of chloroform (the mole fraction is close to 0.35). The nature of the incorporated solvate molecules is determined by high-resolution mass spectrometry, and their quantity is found by thermogravimetry. Original Russian Text",
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Tumanov, NA, Pankrushina, NA, Nefedov, AA & Boldyreva, EV 2012, 'Nanoporous solvate of N,N-phthaloyl-glycine', Journal of Structural Chemistry, VOL. 53, Numéro 3, p. 606-609. https://doi.org/10.1134/S0022476612030298

Nanoporous solvate of N,N-phthaloyl-glycine. / Tumanov, N. A.; Pankrushina, N. A.; Nefedov, A. A.; Boldyreva, E. V.

Dans: Journal of Structural Chemistry, Vol 53, Numéro 3, 05.2012, p. 606-609.

Résultats de recherche: Contribution à un journal/une revueArticle

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AB - N,N-phthaloyl-glycine is synthesized under microwave activation without solvent. Its nanoporous solvate is obtained by recrystallization. The solvate is studied by single crystal and powder XRD, thermogravimetry, and mass spectrometry. The crystals are composed of dimers that form a framework structure with infinite channels of about 4 Å in diameter, containing a non-stoichiometric amount of chloroform (the mole fraction is close to 0.35). The nature of the incorporated solvate molecules is determined by high-resolution mass spectrometry, and their quantity is found by thermogravimetry. Original Russian Text

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