A Simple and Efficient Mechanochemical Route for the Synthesis of Salophen Ligands and of the Corresponding Zn, Ni, and Pd Complexes

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Résumé

A number of salophen ligands and their Zn, Ni, and Pd complexes were synthesized by anefficient one-pot mechanosynthesis protocol. The reaction products were characterized by means ofcomplementary solid-state techniques, i.e., powder X-ray diffraction, single-crystal X-ray diffraction,and solid-state NMR spectroscopy. Four new crystal structures of metal salophen complexes as DMSOsolvates are here reported. The described simple and relatively fast (about 1 h for all derivatives)procedure is a good alternative to classical methods performed in organic solvents.
langue originaleAnglais
Numéro d'article2314
Pages (de - à)2314
Nombre de pages11
journalMolecules
Volume24
Numéro de publication12
Les DOIs
étatPublié - 1 janv. 2019

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