Physico-chimie et caractérisation (PC2)

Equipement/installations: Plateforme technolgique

  • emplacement

    Belgique

Détails des équipements

!!Description

DESCRIPTION
The PC2 Platform is constituted by a large park of instruments including: nuclear magnetic resonance (both liquid and solid state) spectrometers, single-crystal and powder X-ray diffractiometers, instruments for the analysis of the textural properties (N2 physisorption, mercury porosimetry, ...) and for the chemical composition (combustion chemical analysis, ICP, ...) as well as separation techniques (chromatography, centrifugation...)
The combination of these techniques together with the presence of technicians full time dedicated to the analysis of the samples and highly qualified researchers for the development of advanced applications represent a strategic feature of this platform. Among these characterization techniques solid state NMR and X-ray diffraction emerged as advanced tools for characterization.
The platform is active in collaboration with academic teams, both at a national and international level. It also has a tradition of fruitful collaborations with industrial partners, especially in the fields of materials sciences and with the food and pharmacological industries.

EXPERTISE
All the equipment combined with the technical and scientific expertise available at the PC2.

EQUIPMENT

X-RAY DIFFRACTOMETERS
The X-ray diffraction instruments are used for crystal structure determination, crystalline phase identification, size/strain analysis, etc.
• Single-crystal diffractometer Oxford Diffraction Gemini (Mo/Cu radiation, CCD detector)
• Powder diffractometer PANanalytical – X’Pert Pro MRD (Cu radiation, Bragg-Brentano geometry)
• Crystal structure determination, absolute structure, protein crystal screening
• Crystalline phase identification and quantification, size/strain analysis

NMR spectrometers
• Solid-state 500 MHz Bruker Avance (several MAS probes)
• Liquid-state 500 MHz Jeol ECZR (5-mm inverse broadband probe, autosampler)
• Solid-state 400 MHz Varian VNMRS (several static and MAS probes)
• Liquid-state 400 MHz Jeol ECX (5-mm direct broadband probe, autosampler)

Other
• Elemental analysis, centrifugation, gas physisorption, mercury porosimetry.

Empreinte digitale Explorez les domaines de recherche dans lesquels cet équipement a été utilisé. Ces libellés sont générés sur la base des résultats correspondants. Ensemble, ils forment une empreinte digitale unique.

  • Résultat de recherche

    Melamine-based polymer networks enabled N, O, S Co-doped defect-rich hierarchically porous carbon nanobelts for stable and long-cycle Li-ion and Li-Se batteries

    Dong, W. D., Yu, W. B., Xia, F. J., Chen, L. D., Zhang, Y. J., Tan, H. G., Wu, L., Hu, Z. Y., Mohamed, H. S. H., Liu, J., Deng, Z., Li, Y., Chen, L. H. & Su, B. L., 15 janv. 2021, Dans : Journal of Colloid and Interface Science. 582, p. 60-69 10 p.

    Résultats de recherche: Contribution à un journal/une revueArticle

  • Synergistic effects of carbon doping and coating of TiO2 with exceptional photocurrent enhancement for high performance H2 production from water splitting

    Wang, Y., Chen, Y. X., Barakat, T., Wang, T. M., Krief, A., Zeng, Y. J., Laboureur, M., Fusaro, L., Liao, H. G. & Su, B. L., mai 2021, Dans : Journal of Energy Chemistry. 56, p. 141-151 11 p.

    Résultats de recherche: Contribution à un journal/une revueArticle

  • Active faceted Cu2O hollow nanospheres for unprecedented adsorption and visible-light degradation of pollutants

    Yu, W., Liu, J., Yi, M., Yang, J., Dong, W., Wang, C., Zhao, H., Mohamed, H. S. H., Wang, Z., Chen, L., Li, Y. & Su, B. L., 1 avr. 2020, Dans : Journal of Colloid and Interface Science. 565, p. 207-217 11 p.

    Résultats de recherche: Contribution à un journal/une revueArticle

  • Projets

    Activités

    Chromium nitridedeposition onto silicon pyramids for supercapacitor applications

    Emile Haye (Orateur), , Abdelouadoud GUERRA (Orateur), , Amine Achour (Orateur), , Jean-Jacques Pireaux (Orateur), & Stephane Lucas (Orateur)

    9 sept. 2020

    Activité: Types de discours ou de présentationPrésentation orale

    Conférence invitée à l'Université de Toulouse

    Guillaume Berionni (Orateur invité)

    18 déc. 2019

    Activité: Types de discours ou de présentationPrésentation orale

    Glancing angle deposition of CrN film for supercapacitor application.

    Emile Haye (Orateur), , Amine Achour (Orateur), , Abdelouadoud GUERRA (Orateur), , Fatsah MOULAI (Orateur), , Toufik HADJERSI (Orateur), , Rabah Boukherroub (Orateur), , Adriano PANEPINTO (Orateur), , Thierry BROUSSE (Orateur), , Jean-Jacques Pireaux (Orateur), & Stéphane Lucas (Orateur)

    mai 2019

    Activité: Types de discours ou de présentationPrésentation orale