Physico-chimie et caractérisation (PC2)

Equipement/installations: Plateforme technolgique

  • emplacement

    Belgique

Détails des équipements

!!Description

DESCRIPTION
The PC2 Platform is constituted by a large park of instruments including: nuclear magnetic resonance (both liquid and solid state) spectrometers, single-crystal and powder X-ray diffractiometers, instruments for the analysis of the textural properties (N2 physisorption, mercury porosimetry, ...) and for the chemical composition (combustion chemical analysis, ICP, ...) as well as separation techniques (chromatography, centrifugation...)
The combination of these techniques together with the presence of technicians full time dedicated to the analysis of the samples and highly qualified researchers for the development of advanced applications represent a strategic feature of this platform. Among these characterization techniques solid state NMR and X-ray diffraction emerged as advanced tools for characterization.
The platform is active in collaboration with academic teams, both at a national and international level. It also has a tradition of fruitful collaborations with industrial partners, especially in the fields of materials sciences and with the food and pharmacological industries.

EXPERTISE
All the equipment combined with the technical and scientific expertise available at the PC2.

EQUIPMENT

X-RAY DIFFRACTOMETERS
The X-ray diffraction instruments are used for crystal structure determination, crystalline phase identification, size/strain analysis, etc.
• Single-crystal diffractometer Oxford Diffraction Gemini (Mo/Cu radiation, CCD detector)
• Powder diffractometer PANanalytical – X’Pert Pro MRD (Cu radiation, Bragg-Brentano geometry)
• Crystal structure determination, absolute structure, protein crystal screening
• Crystalline phase identification and quantification, size/strain analysis

NMR spectrometers
• Solid-state 500 MHz Bruker Avance (several MAS probes)
• Liquid-state 500 MHz Jeol ECZR (5-mm inverse broadband probe, autosampler)
• Solid-state 400 MHz Varian VNMRS (several static and MAS probes)
• Liquid-state 400 MHz Jeol ECX (5-mm direct broadband probe, autosampler)

Other
• Elemental analysis, centrifugation, gas physisorption, mercury porosimetry.

Empreinte digitale Explorez les domaines de recherche dans lesquels cet équipement a été utilisé. Ces libellés sont générés sur la base des résultats correspondants. Ensemble, ils forment une empreinte digitale unique.

  • Résultat de recherche

    Ethoxycarbonyl functionalized Tröger's base alongside its congener dihydroquinazoline: A trick with crystallization

    Kovalenko, V., Tumanov, N., Vasiutovich, K. & Leyssens, T., févr. 2020, Dans : Chemical Data Collections. 25, 100339.

    Résultats de recherche: Contribution à un journal/une revueArticle

    Accès ouvert
    File
  • 3 Téléchargements (Pure)

    Highly porous hybrid metallosilicate materials prepared by non-hydrolytic sol-gel: Hydrothermal stability and catalytic properties in ethanol dehydration

    Styskalik, A., Kordoghli, I., Poleunis, C., Delcorte, A., Aprile, C., Fusaro, L. & Debecker, D. P., 1 mai 2020, Dans : Microporous and Mesoporous Materials. 297, 110028.

    Résultats de recherche: Contribution à un journal/une revueArticle

  • High performance of 3D silicon nanowires array@CrN for electrochemical capacitors

    Guerra, A., Haye, E., Achour, A., Harnois, M., Hadjersi, T., Colomer, J. F., Pireaux, J. J., Lucas, S. & Boukherroub, R., 17 janv. 2020, Dans : Nanotechnology. 31, 3, p. 035407 8 p., 035407.

    Résultats de recherche: Contribution à un journal/une revueArticle

  • Projets

    Activités

    Conférence invitée à l'Université de Toulouse

    Guillaume Berionni (Orateur invité)

    18 déc. 2019

    Activité: Types de discours ou de présentationPrésentation orale

    Mohamed Ghaffour

    Yves Caudano (Hôte)

    27 nov. 20178 déc. 2017

    Activité: Types d'Accueil d'un visiteurAccueil d'un chercheur étranger

    Abdallah Ouerdane

    Yves Caudano (Hôte)

    27 nov. 201711 déc. 2017

    Activité: Types d'Accueil d'un visiteurAccueil d'un chercheur étranger