Organic-bridged faujasite X zeolites ZOF-X

Bao Lian Su; K. Vause; M. Roussel; L. Shi; X. D. Zou; E. Leonova; M. Edén

doi:10.1016/S0167-2991(07)80889-5

Organic-bridged faujasite X zeolites ZOF-X

Bao Lian Su, K. Vause, M. Roussel, L. Shi, X. D. Zou, E. Leonova, M. Edén

University of Namur

Research output: Contribution in Book/Catalog/Report/Conference proceeding › Chapter

Abstract

Highly thermally stable Faujasite X zeolites with organic-bridged frameworks (ZOF-X) have been for the first time synthesized, in which oxygen atoms in the zeolite frameworks are partially superseded by methylene groups using methylene-bridged bis[triethoxysilyl]methane (BTESM) as a unique silicon source. The presence and the amount of the methylene groups within the framework have been revealed and determined by a series of techniques such as ²⁹Si and ¹³C MAS NMR, XRD, SEM-EDS, FTIR, TG, N₂ adsorption and elemental analysis. The present study showed that the synthesis of ZOF-X materials is quite sensitive to many parameters such as the crystallization and the ageing conditions and finally the batch compositions.

Original language	English
Title of host publication	From Zeolites to Porous MOF Materials
Subtitle of host publication	The 40th Anniversary of International Zeolite Conference
Editors	Ruren Xu, Zi Gao, Jiesheng Chen, Wenfu Yan
Publisher	Elsevier Inc.
Pages	539-545
Number of pages	7
Edition	A
ISBN (Print)	0444530681, 9780444530684
DOIs	https://doi.org/10.1016/S0167-2991(07)80889-5
Publication status	Published - 1 Jan 2007

Publication series

Name	Studies in Surface Science and Catalysis
Number	A
Volume	170
ISSN (Print)	0167-2991

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10.1016/S0167-2991(07)80889-5

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Su, B. L., Vause, K., Roussel, M., Shi, L., Zou, X. D., Leonova, E., & Edén, M. (2007). Organic-bridged faujasite X zeolites ZOF-X. In R. Xu, Z. Gao, J. Chen, & W. Yan (Eds.), From Zeolites to Porous MOF Materials : The 40th Anniversary of International Zeolite Conference (A ed., pp. 539-545). (Studies in Surface Science and Catalysis; Vol. 170, No. A). Elsevier Inc.. https://doi.org/10.1016/S0167-2991(07)80889-5

Su, Bao Lian ; Vause, K. ; Roussel, M. ; Shi, L. ; Zou, X. D. ; Leonova, E. ; Edén, M. / Organic-bridged faujasite X zeolites ZOF-X. From Zeolites to Porous MOF Materials : The 40th Anniversary of International Zeolite Conference. editor / Ruren Xu ; Zi Gao ; Jiesheng Chen ; Wenfu Yan. A. ed. Elsevier Inc., 2007. pp. 539-545 (Studies in Surface Science and Catalysis; A).

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abstract = "Highly thermally stable Faujasite X zeolites with organic-bridged frameworks (ZOF-X) have been for the first time synthesized, in which oxygen atoms in the zeolite frameworks are partially superseded by methylene groups using methylene-bridged bis[triethoxysilyl]methane (BTESM) as a unique silicon source. The presence and the amount of the methylene groups within the framework have been revealed and determined by a series of techniques such as 29Si and 13C MAS NMR, XRD, SEM-EDS, FTIR, TG, N2 adsorption and elemental analysis. The present study showed that the synthesis of ZOF-X materials is quite sensitive to many parameters such as the crystallization and the ageing conditions and finally the batch compositions.",

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Su, BL, Vause, K, Roussel, M, Shi, L, Zou, XD, Leonova, E & Edén, M 2007, Organic-bridged faujasite X zeolites ZOF-X. in R Xu, Z Gao, J Chen & W Yan (eds), From Zeolites to Porous MOF Materials : The 40th Anniversary of International Zeolite Conference. A edn, Studies in Surface Science and Catalysis, no. A, vol. 170, Elsevier Inc., pp. 539-545. https://doi.org/10.1016/S0167-2991(07)80889-5

Organic-bridged faujasite X zeolites ZOF-X. / Su, Bao Lian; Vause, K.; Roussel, M.; Shi, L.; Zou, X. D.; Leonova, E.; Edén, M.

From Zeolites to Porous MOF Materials : The 40th Anniversary of International Zeolite Conference. ed. / Ruren Xu; Zi Gao; Jiesheng Chen; Wenfu Yan. A. ed. Elsevier Inc., 2007. p. 539-545 (Studies in Surface Science and Catalysis; Vol. 170, No. A).

Research output: Contribution in Book/Catalog/Report/Conference proceeding › Chapter

TY - CHAP

T1 - Organic-bridged faujasite X zeolites ZOF-X

AU - Su, Bao Lian

AU - Vause, K.

AU - Roussel, M.

AU - Shi, L.

AU - Zou, X. D.

AU - Leonova, E.

AU - Edén, M.

PY - 2007/1/1

Y1 - 2007/1/1

N2 - Highly thermally stable Faujasite X zeolites with organic-bridged frameworks (ZOF-X) have been for the first time synthesized, in which oxygen atoms in the zeolite frameworks are partially superseded by methylene groups using methylene-bridged bis[triethoxysilyl]methane (BTESM) as a unique silicon source. The presence and the amount of the methylene groups within the framework have been revealed and determined by a series of techniques such as 29Si and 13C MAS NMR, XRD, SEM-EDS, FTIR, TG, N2 adsorption and elemental analysis. The present study showed that the synthesis of ZOF-X materials is quite sensitive to many parameters such as the crystallization and the ageing conditions and finally the batch compositions.

AB - Highly thermally stable Faujasite X zeolites with organic-bridged frameworks (ZOF-X) have been for the first time synthesized, in which oxygen atoms in the zeolite frameworks are partially superseded by methylene groups using methylene-bridged bis[triethoxysilyl]methane (BTESM) as a unique silicon source. The presence and the amount of the methylene groups within the framework have been revealed and determined by a series of techniques such as 29Si and 13C MAS NMR, XRD, SEM-EDS, FTIR, TG, N2 adsorption and elemental analysis. The present study showed that the synthesis of ZOF-X materials is quite sensitive to many parameters such as the crystallization and the ageing conditions and finally the batch compositions.

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BT - From Zeolites to Porous MOF Materials

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PB - Elsevier Inc.

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Su BL, Vause K, Roussel M, Shi L, Zou XD, Leonova E et al. Organic-bridged faujasite X zeolites ZOF-X. In Xu R, Gao Z, Chen J, Yan W, editors, From Zeolites to Porous MOF Materials : The 40th Anniversary of International Zeolite Conference. A ed. Elsevier Inc. 2007. p. 539-545. (Studies in Surface Science and Catalysis; A). https://doi.org/10.1016/S0167-2991(07)80889-5