Effect of nonionic surfactants on structure, texture, and morphology of titania-doped YSZ

N. Cioatera, V. Pârvulescu, B.-L. Su

Research output: Contribution to journalArticle

Abstract

The effect of nonionic surfactant structure and concentration on the structural and textural properties, as well as on morphology of titania-doped YSZ (yttria-stabilized zirconia) (TYZ) prepared by the citrate polymeric method is investigated in order to design the optimal conditions for the synthesis of highly structured materials. The calcined powders were characterized by wide- and small-angle X-ray diffraction (wa-XRD and sa-XRD), N adsorption-desorption, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Mesoporous ceramic materials have been obtained when 8 vol% alkyl poly(oxyethylene) surfactants were added in the reaction mixture, samples having a BET surface area of about 106 m g.
Original languageEnglish
Pages (from-to)697-701
Number of pages5
JournalMaterials Chemistry and Physics
Volume120
Issue number2-3
DOIs
Publication statusPublished - 15 Apr 2010

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Mesoporous materials
Yttria stabilized zirconia
Nonionic surfactants
Ceramic materials
yttria-stabilized zirconia
Surface-Active Agents
Citric Acid
Powders
Desorption
Surface active agents
textures
titanium
Titanium
Textures
surfactants
Transmission electron microscopy
Adsorption
X ray diffraction
Scanning electron microscopy
citrates

Cite this

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abstract = "The effect of nonionic surfactant structure and concentration on the structural and textural properties, as well as on morphology of titania-doped YSZ (yttria-stabilized zirconia) (TYZ) prepared by the citrate polymeric method is investigated in order to design the optimal conditions for the synthesis of highly structured materials. The calcined powders were characterized by wide- and small-angle X-ray diffraction (wa-XRD and sa-XRD), N adsorption-desorption, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Mesoporous ceramic materials have been obtained when 8 vol{\%} alkyl poly(oxyethylene) surfactants were added in the reaction mixture, samples having a BET surface area of about 106 m g.",
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Effect of nonionic surfactants on structure, texture, and morphology of titania-doped YSZ. / Cioatera, N.; Pârvulescu, V.; Su, B.-L.

In: Materials Chemistry and Physics , Vol. 120, No. 2-3, 15.04.2010, p. 697-701.

Research output: Contribution to journalArticle

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