A dinitrobenzoate derivative of an α-methoxy-γ-hydroxysilane

G. Baudoux, B. Norberg, J. Bousbaa, A. Krief, G. Evrard

Research output: Contribution to journalArticle

Abstract

The structure of (2S*, 4S*)-4-methoxy-4-phenyl-4-(trimethylsilyl)-2-butyl 3,5-dinitrobenzoate, CHNOSi, is presented and discussed. The compound was synthesized by a stereoselective [1-4] retro-Brook reaction, followed by acylation using 3,5-dinitrobenzoyl chloride. The Si-O chain adopts a sterically hindered conformation resembling a five-membered ring.
Original languageEnglish
Pages (from-to)1944-1945
Number of pages2
JournalActa crystallographica Section C: Crystal Structure communications
Volume54
Issue number12
Publication statusPublished - 15 Dec 1998

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